Emrys Synthesizer

Fig. 4. Monomode microwave reactor with integrated robotic platform for automated use (left). A liquid handler allows dispensing of reagents into Teflon-sealed reaction vials, while a gripper moves each vial in and out of the microwave cavity after irradiation. The instrument processes up to 120 reactions per run with a maximum throughput of 12-15 reactions/h. The temperature is measured by an IR sensor on the outside of the reaction vessel. Details of the cavity/gripper (top right) and reaction vials (bottom right) are also displayed (Emrys Synthesizer, Personal Chemistry AB). Reprinted with permission from Wiley-VCH.41 (See color insert.)...

Wilson and coworkers described a custom-made flow-reactor for the Bio-tage Emrys Synthesizer single-mode batch reactor (Fig. 21) that was fitted with a glass-coiled flow cell [67]. The flow cell was inserted into the cavity from the bottom of the instrument and the system was operated either under... 

Fig. 21 Flow reactor applied with the Emrys Synthesizer. Reproduced with permission from [67]...

Baxendale and Ley [60] employed the Smith Synthesizer as well as the Emrys Optimizer from Biotage [59] for conducting neat KOf-Bu mediated trimerizations of various liquid nitriles to give aryl- and alkyl-substituted 4-... 

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