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Dinitrophenyl derivatives, of amines

Fig. 5.8. Gas chromatogram of a mixture of 2,4-dinitrophenyl derivatives of amines. Peaks 1 = ammonia 2 = diethylamine 3 = isopropylamine 4 = rm.-butylamine 5 = sec.-butylamine 6 = iso-amylamine 7 = n-amylamine 8 = TMS-ethanolamine 9 = aniline 10 = cyclohexylamine 11 = benzyl-amine 12 = (3-phenylethylamine. Conditions glass column, 3 m X 3 mm I.D., 10% SE-30 on Chromo-sorb W (60-80 mesh, AW, silanized) nitrogen flow-rate, 35 ml/min temperature programme, 2°C/min (190-220°C), 3°C/min (220-250°C). (Reproduced from J. Chromatogr., 88 (1974) 373, by courtesy of S. Baba.)... Fig. 5.8. Gas chromatogram of a mixture of 2,4-dinitrophenyl derivatives of amines. Peaks 1 = ammonia 2 = diethylamine 3 = isopropylamine 4 = rm.-butylamine 5 = sec.-butylamine 6 = iso-amylamine 7 = n-amylamine 8 = TMS-ethanolamine 9 = aniline 10 = cyclohexylamine 11 = benzyl-amine 12 = (3-phenylethylamine. Conditions glass column, 3 m X 3 mm I.D., 10% SE-30 on Chromo-sorb W (60-80 mesh, AW, silanized) nitrogen flow-rate, 35 ml/min temperature programme, 2°C/min (190-220°C), 3°C/min (220-250°C). (Reproduced from J. Chromatogr., 88 (1974) 373, by courtesy of S. Baba.)...
See other pages where Dinitrophenyl derivatives, of amines is mentioned: [Pg.105]   
See also in sourсe #XX -- [ Pg.1276 ]

See also in sourсe #XX -- [ Pg.1276 ]



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