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2,2-difluoro-5-phenyl

US patent 6,713,481, Crystalline antifungal polymorph [104]. This patent discloses the crystalline polymorph Form I of ( )-4-[4-[4-[4-[[(2R-cA)-5-(2,4-difluoro-phenyl)tetrahydro-5-( 1H-1,2,4-triazol- l-ylmethyl)furan-3-yl]methoxy]phenyl]-1 -piper azinyl]phenyl-2,4-dihydro-2-[(S)-l-ethyl-2(S)-hydroxylpropyl]-3H-l,2,4-triazol-3-one,... [Pg.277]

Difluoro(phenyl)methyl Methyl Ether Typical Procedure 57... [Pg.418]

Diethyl(trifluoromethyl)amine and [Difluoro(phenyl)methyl)(dimethyl)ainine... [Pg.541]

Diethyl(trifluoromethyl)amine (19) and [difluoro(phenyl)methyl](dimethyl)amine (21) are synthesized from the corresponding diethylformamide (18) and N, /V-dimethylbenzamide (20), respectively. The fluorination is achieved with sulfur tetrafluoride in the presence of potassium fluoride at 150l,C.36... [Pg.541]

Diethyl(trifluoromethyl)amine (19 14.1 g, 0.1 mol) was added dropwise to i-PrOH (22 6g, 0.1 mol) at 40CC with stirring, an exothermic reaction occurred and the mixture was brought to reflux. Once the addition was complete the mixture was stirred for a further 15 min. The volatile 2-fluoropropane (23) which evolved during the course of the reaction was condensed into a cold trap at — 78°C yield 4.6 g (74%). An identical yield was obtained when the same procedure was performed with [difluoro(phenyl)-methyl](dimethyl)amine (21) instead of 19. [Pg.542]

To PhBCl2 (2 g, 13 mmol) in a 50-mL round-bottomed flask equipped with a short Vigreux column and a distillation head was added NaBF4 (3 g, 28 mmol) and the mixture was heated until the product distilled. The distillate [difluoro(phenyl)borane] distilled at 78 JC under atmospheric pressure. [Pg.614]

Thallium Difluoro-phenyl- ElOa. 640 (20Ac 2F) c h5f3n2o,... [Pg.623]

Methane Chloro-difluoro-phenyl-ElOa. 5f. (History). 519/524/643 (2Cl - 2D... [Pg.636]

Ethanoate Ethyl Difluoro-phenyl-ElOa, 415 (CO -> CF2) ElOb, 178 (CO -> CF,)... [Pg.674]

Silane tert.-Butyl-difluoro-phenyl-ElOa, 613(2C1 2F)... [Pg.677]

Methane Difluoro-phenyl-(trime-thylsilyl-methoxy)- ElOa, 418 (CS - CF2)... [Pg.686]

Methane (4-Chloro-plienyl)-difluoro-phenyl- ElOb, 214... [Pg.698]

Difluoro-phenyl)-2-(7-methyl-lH-indazol-3-yl)-thiazol-4-yl] -(4-methyl-piperazin-1 -yl) -methanone 1 H A-n. VS F w. NY... [Pg.117]

Methane Chloro-difluoro-phenyl-E10 (CC13 - CC1F2)... [Pg.349]


See other pages where 2,2-difluoro-5-phenyl is mentioned: [Pg.875]    [Pg.875]    [Pg.1980]    [Pg.191]    [Pg.120]    [Pg.1263]    [Pg.1263]    [Pg.46]    [Pg.388]    [Pg.614]    [Pg.623]    [Pg.623]    [Pg.623]    [Pg.637]    [Pg.663]    [Pg.686]    [Pg.699]    [Pg.706]    [Pg.709]    [Pg.145]    [Pg.125]    [Pg.126]    [Pg.642]    [Pg.875]    [Pg.231]    [Pg.1034]    [Pg.36]    [Pg.2188]    [Pg.259]   
See also in sourсe #XX -- [ Pg.828 ]

See also in sourсe #XX -- [ Pg.828 ]




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1.1- difluoro-2-phenyl-2 ethene

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