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Deacetylation reductive iodination

Olefin addition. Addition of iodine and A -cholestene to a solution of silver trifluoroacetate in methylene chloride generates iodine trifluoroacetate which adds to the olefin to give 3a-iodo-2 -trifluoroacetatoxycholestane in 72% yield. Lithium aluminum hydride effects reduction and deacetylation to cholestane-2/3-ol. D. E. Janssen and C. V. Wilson, Org. Syn., Coll. Vol., 4,547 (1963)... [Pg.1243]

See other pages where Deacetylation reductive iodination is mentioned: [Pg.66]    [Pg.66]    [Pg.298]    [Pg.69]    [Pg.594]    [Pg.581]    [Pg.420]    [Pg.132]   
See also in sourсe #XX -- [ Pg.6 ]



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Deacetylated

Iodine reduction

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