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Cyclophellitol aziridine

Cyclophellitol Aziridine Is a Broad-Spectrum Activity-Based Retaining p-Exoglucosidase Probe... [Pg.198]

Figure 13.5 Synthesis of broad-spectrum retaining fi-exoglucoside probe cyclophellitol aziridine 13 and IS. (a) (i) CCIjCN, DBU (1,8-diazabicyclo[5.4.0]undec-7-ene), CHjClj, 0°C, 2h, (ii) followed by the addition of HjO, NaHCOj, Ij, 18h, (b) (i) 37% HCI, MeOH, 3.5 h, (ii) 37% HCI, dioxane, 60 °C, 1 h, (ill) NaHCOj MeOH, 4 days (over five steps 60%), (c) (i)... Figure 13.5 Synthesis of broad-spectrum retaining fi-exoglucoside probe cyclophellitol aziridine 13 and IS. (a) (i) CCIjCN, DBU (1,8-diazabicyclo[5.4.0]undec-7-ene), CHjClj, 0°C, 2h, (ii) followed by the addition of HjO, NaHCOj, Ij, 18h, (b) (i) 37% HCI, MeOH, 3.5 h, (ii) 37% HCI, dioxane, 60 °C, 1 h, (ill) NaHCOj MeOH, 4 days (over five steps 60%), (c) (i)...
See other pages where Cyclophellitol aziridine is mentioned: [Pg.200]    [Pg.200]    [Pg.2347]    [Pg.377]    [Pg.203]    [Pg.236]   
See also in sourсe #XX -- [ Pg.198 , Pg.200 ]



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