Melting point compounds

To a mixture of 60 cc of benzene, 40 cc of pyridine and 17 g of hydrochloric acid salt of nicotinic acid chloride, was added 4.5 g of 2,2,6,6-tetramethylolcyclohexanol, and the whole mixture was refuxed at 75°C to 80°C for 2.5 hours. After the mixture was cooled water was added. Precipitate formed was separated by filtration, washed thoroughly with water and dried. Recrystallization from dilute acetic acid gave 14gof the final compound, melting point 177°Cto 180°C. 

Compound Melting point K Boiling point K Specific conductance Ohm 1 cm 1 at 1200 K Decomposition potential E at 1073 K ... 

Compound Melting point (°C) Rotation Md (degrees) Solvent References... 

Compound Melting Point (°C) Boiling Point (°C) Dipole Moment (D)... 

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