Bis tetrabutylammonium Octachloroditechnetate III

The reaction is performed in a 250 mL round-bottomed flask equipped with a three-hole rubber stopper. A portion of (n-Bu4N)TcOCl4 (933 mg, 1.866 mmol) is 

TABLE 1. Optical Absorption Spectra of M2Clg (M = Tc, Re) in Degassed Dichloromethane.  

Sattelberger, in Multiple Bonds Between Metal Atoms, 3rd ed., F. A. Cotton, C. A. Murillo, and R. A. Walton, eds.. Springer, New York, 2005. 

Schwochau, K. Hedwig, H. J. Schenk, and O. Greis, Inorg. Nucl. Chem. Lett. 13, 77 (1977). 

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