2-benzoyloxy-3-chloropropyl

Bis[2-benzoyloxy-3-chloropropyl] Ditellurium1 In a 250 ml separatory funnel are placed 0.80 g (1.85 mmol) of 2-benzoyloxy-3-chloropropyl tellurium trichloride, 40 ml of dichloromethane, and 30 ml of 20% (w/v) aqueous sodium sulfide nonahydrate solution. The mixture is shaken until all solids have dissolved, the organic layer is separated, dried, and the solvent evaporated. The product is purified by passing it through a short column of silica with dichloromethane as the mobile phase. The orange-red colored fractions are evaporated to leave a red oil yield 0.48 g (80%). 

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See also in sourсe #XX -- [ ]

See also in sourсe #XX -- [ ]

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