Acetylene dideuterio

Generation of an Acetylene-Titanium Alkoxide Complex, Preparation of (Z)-1,2-Dideuterio-1 -(trimethylsilyl)-l -hexene. 

GENERATION OF AN ACETYLENE-TITANIUM ALKOXIDE COMPLEX PREPARATION OF (Z)-l,2-DIDEUTERIO-l-(TRIMETHYLSILYL)-l-HEXENE... 

Further, hydrolysis of some carbides with D20 leads to important fundamental compounds with deuterium labeling. For example, dideuterio-acetylene is obtained from CaC2f50 tetradeuteriomethane from A14C3,51 and perdeuterated allene from Mg2C3 at about 350° 52... 

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